HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131711967, compound → 4-Chlorobenzyl alcohol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131711967 | HCID 131711967 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 4-Chlorobenzyl alcohol | HCID 13397 | 82.1% |
Reaction Steps
100 ml of glacial acetic acid and 5 g of 5% Pd on C are added to a solution of p-chlorobenzoyl-ethyl carbonate (22.8 g=0.1 moles). The mixture is reduced in a PARR apparatus for 10 hours at 60° and under a pressure of 200 psi (14 atm) of H2. We proceed as in Example II. We obtain 11.7 g (82%) of a product having the following characteristics:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04239702 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-6f6d8ef2ec9e400f986c7872f65b62ff |
| Source note | uspto-grants-1980_12 |