HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 70597034, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 70596907 | HCID 70596907 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 70597034 | HCID 70597034 | — |
Reaction Steps
A solution of 2.63 g of 1-isopropylimino-3-p-biphenylyl-2-butene (obtainable from 3-p-biphenylyl-2-butenal and isopropylamine) in 20 ml of absolute ether is added dropwise to a solution of 0.6 g of LiAlH4 in 20 ml of absolute ether. The mixture is then boiled for 5 hours, water is added carefully and the mixture is worked up in the customary manner to give 1-isopropylamino-3-p-biphenylyl-2-butene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04239759 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-d43e9b639c4140a9827c21e5c27a6327 |
| Source note | uspto-grants-1980_12 |