HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phthalimide potassium salt → HCID 70595721, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phthalimide potassium salt | HCID 24194345 | — |
| Reactant | HCID 70595719 | HCID 70595719 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 70595721 | HCID 70595721 | — |
Reaction Steps
A mixture of 2.6 g of 1-chloro-3-p-biphenylyl-butan-3-ol, 2.04 g of potassium phthalimide and 40 ml of DMF is heated at 110° for 1.5 hours. After cooling, the mixture is worked up in the customary manner to give 1-phthalimido-3-p-biphenylyl-butan-3-ol, m.p. 153°-155°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04239759 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-91344bebcd91471284b2d02a757b56cc |
| Source note | uspto-grants-1980_12 |