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HRID1733052

反应详情

EQUATION

反应方程式

HRID 1733052 的结构方程式

REACTANTS

反应物

2
结构：O=C1NC(=O)c2ccccc21.[K]
HCID24194345

未命名化合物

结构：CC(O)(CCCl)c1ccccc1-c1ccccc1
HCID70595719

未命名化合物

PRODUCTS

生成物

1
结构：CC(O)(CCN1C(=O)c2ccccc2C1=O)c1ccccc1-c1ccccc1
HCID70595721

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

A mixture of 2.6 g of 1-chloro-3-p-biphenylyl-butan-3-ol, 2.04 g of potassium phthalimide and 40 ml of DMF is heated at 110° for 1.5 hours. After cooling, the mixture is worked up in the customary manner to give 1-phthalimido-3-p-biphenylyl-butan-3-ol, m.p. 153°-155°.

WORKUP

后处理

  1. temperatureis heated at 110° for 1.5 hours
  2. temperatureAfter cooling