HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 3-(4'-Fluoro-4-biphenylyl)butylamine, hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1-Phthalimido-3-(4'-fluoro-4-biphenylyl)butane | HCID 20301979 | — |
| Product | 3-(4'-Fluoro-4-biphenylyl)butylamine, hydrochloride | HCID 20302716 | — |
Reaction Steps
37.3 g of 1-phthalimido-3-(4'-fluoro-4-biphenylyl)butane are boiled for 6 hours with 400 ml of 20% aqueous hydrochloric acid, evaporated and worked up using sodium hydroxide solution and ether to give 3-(4'-fluoro-4-biphenylyl)butylamine, hydrochloride, m.p. 222°-224°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04239759 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-2608ab0b49d742eb968b25e2e0900b6c |
| Source note | uspto-grants-1980_12 |