HuagongsheHuagongshe Chemistry Print Report · For research reference only
Peracetic Acid → HCID 12637736, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Peracetic Acid | HCID 6585 | — |
| Reactant | 4-Nitro-6-(trifluoromethyl)-1,3-benzodithiole-2-thione | HCID 12637734 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 12637736 | HCID 12637736 | — |
Reaction Steps
To a stirred solution of 7.35 g., (24.7 mmoles) of 4-nitro-6-trifluoromethyl-1,3-benzodithiole-2-thione in 150 ml. of chloroform was added dropwise a solution of 5.17 g., (24.7 mmoles) of 40% peracetic acid in 50 ml. of chloroform over a period of 20 minutes, the temperature being maintained at 8°-12° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04240821 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-1c86db5ac56747db9df172dd3dc874dc |
| Source note | uspto-grants-1980_12 |