Methylamine → HCID 20300367, compound

Participants

Reaction Steps

A solution of 7.8 g (0.041 mole) of 3-cyano-4-tert.-butyl-fur-2-yl isocyanate in 30 ml of toluene was added dropwise to a solution of 1.6 g (0.052 mole) of methylamine in 30 ml of toluene. Thereafter, the mixture was worked up by concentrating it under reduced pressure and recrystallizing the residue from toluene. 6.8 g of 1-(3-cyano-4-tert.-butyl-fur-2-yl)-3-methylurea of melting point 163° C. were obtained in this manner.

Provenance & Evidence