HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20300399, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1-Chloro-2-nitrobenzene | HCID 6945 | — |
| Reactant | 3-Pentanamine | HCID 12019 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20300399 | HCID 20300399 | 91% |
Reaction Steps
A solution of 158 grams of o-nitrochlorobenzene and 260 grams of 1-ethylpropylamine are refluxed together for 5 days. The solution is cooled and 500 ml. of water is added. Concentrated hydrochloric acid (10 milliliters) is added and the product separates out as an oil. The product is extracted with chloroform (2×200 milliliters), the extractions dried over MgSO4 and evaporated to yield 190 grams (91%) of product as an oil. The analytical sample is prepared by distillation of the crude oil, b.p. 1.8 mm Hg=148° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04240822 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-eb0f84574c864e4398ebdad0dab1de42 |
| Source note | uspto-grants-1980_12 |