HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trichloromethanesulfenyl chloride → HCID 20300405, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trichloromethanesulfenyl chloride | HCID 11666 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 178526563 | HCID 178526563 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20300405 | HCID 20300405 | — |
Reaction Steps
A solution of 10.2 grams of the sodium salt of 4-nitrobenzotriazole, 6 milliliters of trichloromethylsulfenyl chloride and 100 milliliters of water is stirred at 5° C. for 1 hour. The brown solid is collected by filtration and washed with ethyl ether. The crude product weighs 9.3 grams (51%) and recrystallized from carbon tetrachloride, m.p. 136.5°-137.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04240822 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-23248100907e47ebab737027444dbd28 |
| Source note | uspto-grants-1980_12 |