Allylamine → HCID 53732913, compound

HRID 1733246Notes

Reaction equation

HRID 1733246 reaction equation
O=[CH:2][C@@H:3]([C@H:5]([C@H:7]([CH2:9][OH:10])[OH:8])[OH:6])[OH:4].[CH2:11]([NH2:14])[CH:12]=[CH2:13].[Cl:15][CH2:16][CH2:17][N:18]=[C:19]=[O:20]>>[Cl:15][CH2:16][CH2:17][NH:18][C:19]([N:14]([CH2:11][CH:12]=[CH2:13])[CH:9]1[O:10][CH2:2][C@H:3]([OH:4])[C@H:5]([OH:6])[C@H:7]1[OH:8])=[O:20]

Participants

4

Reactant 3

HCID 7853AllylamineHCID 160352-Chloroethyl isocyanateHCID 5460291aldehydo-L-arabinose

Product 1

HCID 53732913HCID 53732913, compoundYield 62.3%

Procedure

4.5 g of L-arabinose, 2.5 g of 2-propenylamine and 3.5 g of 2-chloroethyl isocyanate are treated in the same manner as described in Example 31-(1). 5.5 g of 1-(2-chloroethyl)-3-(2-propenyl)-3-(L-arabinopyranosyl)urea are thereby obtained as colorless powder.

Sources & evidence

ORD record
ord-d3779bacaf7f45dba5bbbdaefa62f7f5
Source dataset
uspto-grants-1980_12
Patent number
US04241052

Reaction notes

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