Methyl iodide → HCID 178460710, compound

Participants

Reaction Steps

To a solution of 1-iminophenylmethyl-2-(3-carbomethoxythioureido)-4-propylthiobenzene (3.88 g.; 0.01 mol) in acetone (40 ml.) and water (10 ml.) there is added calcium hydroxide (0.74 g.; 0.01 mol). The mixture is stirred at room temperature for 4 hours and then is added methyl iodide (1.42 g.; 0.01 mol). The mixture is stirred at room temperature for 4 hours and the precipitate collected and dried to afford 1-iminophenylmethyl-2-(3-carbomethoxy-S-methylisothioureido)-4-propylthiobenzene.

Provenance & Evidence