Methanol → HCID 86737401, compound

Participants

Reaction Conditions

Reaction Steps

To a suspension of 2-(3-carbomethoxy thioureido)-4-propylthioaniline (9.0 g; 0.03 mole) in methanol (100 ml) cooled to 10° C., there is added p=anisaldehyde (4.08 g; 0.03 mole). The mixture is stirred at 10° C. for 1 hr. and at room temperature for 18 hrs. The suspension that forms is vacuum filtered and the filter cake air dried to afford 1-imino-(4-methoxy)phenylmethyl-2-(3-carbomethoxythioureido)-4-propylthiobenzene (9.9 g,; 79%), m.p. 141°-144° C.

Provenance & Evidence