Hydrochloric Acid → HCID 20299085, compound

Participants

Reaction Conditions

Reaction Steps

500 ml of a 10% sodium carbonate solution was added to a solution of the oil of Step C in 250 ml of methanol and the mixture was stirred for 3 hours at 60° C. and was then cooled to room temperature. 100 ml of 20% hydrochloric acid were added to the mixture which was then extracted with chloroform. The organic phase was evaporated to dryness under reduced pressure and the residue was triturated with petroleum ether to obtain 40 g of 2-hexyl-4-(S-methyl-N-tosyl-sulfonimidoyl)-phenol melting at 109°-110° C.

Provenance & Evidence