Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | HCID 86737403 | HCID 86737403 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20299085 | HCID 20299085 | 89.6% |
Reaction Steps
A suspension of 0.8 g of the product of Step C, 30 ml of a saturated sodium carbonate solution and 15 ml of ethanol was stirred at 50° C. for 15 minutes and the solution was cooled in water. The mixture was acidified with concentrated hydrochloric acid and was extracted with ether. The decanted organic phase was evaporated to dryness to obtain 0.65 g of 2-hexyl-4-(S-methyl-N-tosyl-sulfonimidoyl)-phenol which after crystallization from an ether-petroleum ether mixture melted at 107°-109° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04242267 |
|---|
| Source dataset | uspto-grants-1980_12 |
|---|
| ORD ID | ord-fdac9d2f53b042ed964b0e534aea35c9 |
|---|
| Source note | uspto-grants-1980_12 |
|---|
