HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Sodium 4-chlorophenolate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 4-Chlorophenol | HCID 4684 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Sodium 4-chlorophenolate | HCID 23666363 | — |
Reaction Steps
A large batch of sodium p-chlorophenoxide salt was prepared by the reaction of 529.4 grams (4.12 moles) of p-chlorophenol with 99.0 grams (4.12 moles) of sodium hydride in THF at room temperature. A light yellow solution was obtained after 2 hours. A sample of the salt was neutralized with HCl and analyzed. The analysis showed 100% p-chlorophenol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04242493 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-b6a20a2320bd4858b19b7c49fa3ded6f |
| Source note | uspto-grants-1980_12 |