Furfural → HCID 86736803, compound

HRID 1733547Notes

Reaction equation

HRID 1733547 reaction equation
[NH2:1][C:2]([NH2:4])=[S:3].[Si:5]([O-:9])([O-:8])([O-:7])[O-:6].[Na+].[Na+].[Na+].[Na+].[CH:14](=[O:20])[C:15]1[O:19][CH:18]=[CH:17][CH:16]=1>>[Si:5]([OH:9])([OH:8])([OH:7])[OH:6].[NH2:1][C:2]([NH2:4])=[S:3].[CH:14](=[O:20])[C:15]1[O:19][CH:18]=[CH:17][CH:16]=1

Participants

4

Reactant 3

HCID 7362FurfuralHCID 26051Sodium orthosilicateHCID 2723790Thiourea

Product 1

HCID 86736803HCID 86736803, compound

Procedure

About 1 mol of thiourea (Component B), 1 mol of hydrated silica (Component A), 0.5 mol of sodium silicate (Component A) and 2 mols of furfural (Component C) are mixed, then heated to 60° C. to 100° C. for 20 to 120 minutes, thereby producing a poly(furfural thiourea silicate) resinous product.

Workup

  1. temperatureheated to 60° C. to 100° C. for 20 to 120 minutes

Sources & evidence

ORD record
ord-289709aeb8be40e1b6557740e3729bcc
Source dataset
uspto-grants-1980_12
Patent number
US04242497

Reaction notes

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