Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 20300059 | HCID 20300059 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20300060 | HCID 20300060 | 82% |
Reaction Steps
Next a mixture of 1.96 g (0.01 mole) of ethyl-3-(3-oxo-2-pyridazinyl)propionate and 20 ml of methylamine (30% ethanol solution was stirred at 40° C. for 30 hours and distilled to give white crystals. Recrystallization from ethanol gave 1.6 g (82% yield of N-methyl-3-(3-oxo-2-pyridazinyl)propionamide, m.p. 94°-96° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04242512 |
|---|
| Source dataset | uspto-grants-1980_12 |
|---|
| ORD ID | ord-73bc2c82c892427582a9a3e94637d11d |
|---|
| Source note | uspto-grants-1980_12 |
|---|
