Phosphorus oxychloride → HCID 20296367, compound
Reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([C:9]2[CH:10]=[CH:11][C:12](=O)[NH:13][CH:14]=2)[CH:6]=[CH:7][CH:8]=1.P(Cl)(Cl)([Cl:18])=O>>[Cl:18][C:12]1[CH:11]=[CH:10][C:9]([C:5]2[CH:6]=[CH:7][CH:8]=[C:3]([O:2][CH3:1])[CH:4]=2)=[CH:14][N:13]=1Participants
3
Procedure
In the manner described in Example 26, a mixture of 5-(3-methoxyphenyl)-2(1H)-pyridinone and phosphorus oxychloride yields the product of the Example.
Workup
- customyields the product of the Example
Sources & evidence
- ORD record
- ord-a15cb652aded4304ac43bf876c13508e
- Source dataset
- uspto-grants-1980_12
- Patent number
- US04242515
Reaction notes
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