Nitric Acid → HCID 19438795, compound

Participants

Reaction Steps

1-Ethoxalylamino-4-(1H-imidazol-1-yl)-benzene (16 g; 61.8 mmol) was added gradually to 100 ml nitric acid (d=1.52) at 0° C. Stirring was continued at 0° C. for 1 h, and then the reaction mixture was poured into ice-water to give the title compound (18 g; 80%) as a nitric acid salt. M.p. 180° C. (decomp.).

Provenance & Evidence