Ethoxalyl chloride → HCID 19438794, compound

Participants

Reaction Steps

To a solution of 14.5 g (~50.7 mmol) of 4-amino-2-(2-methyl-1H-imidazol-1-yl)-5-nitrobenzotrifluoride in 200 ml dry pyridine was added dropwise 11,3 ml (~102 mmol) ethoxalyl chloride, and stirring was continued overnight at room temperature. The reaction mixture was filtered and the filtrate was evaporated to give the title compound as a crude oil (19 g).

Provenance & Evidence