HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridinium chloride → HCID 19438824, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Reactant | HCID 19438846 | HCID 19438846 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 19438824 | HCID 19438824 | — |
Reaction Steps
A mixture of 2.1 g of 1-[4-(5-methoxyindol-3-yl)butyl]-4-(chroman-6-yl)piperazine [can be prepared according to Example 1], 1.8 g of pyridine hydrochloride and 50 ml of pyridine is boiled for 3 hours. It is cooled and evaporated, and the residue is worked up in the customary manner and gives 1-[4-(5-hydroxyindol-3-yl)-butyl]-4-(chroman-6-yl)piperazine, m.p. 220°-222°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05532241 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-1562ee5110704344812232473fc29538 |
| Source note | uspto-grants-1996_07 |