HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 19699051, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | [1,1'-Biphenyl]-2-carbonyl chloride | HCID 12563768 | — |
| Reactant | HCID 19699137 | HCID 19699137 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19699051 | HCID 19699051 | — |
Reaction Steps
As described for Example 1, a solution of 2 mmol of 4-(4-aminobenzoyl)-4,5-dihydropyrazolo[3,4-d]pyrido[2,3-b]azepine and 10 mmol of triethylamine is stirred with [1,1'-biphenyl]-2-carbonyl chloride in dichloromethane for 16 hours at room temperature. The initial solid is stirred with 1N NaOH in methanol as described in Example 1 to give the product as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05532235 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-4a2df769fc3a48c680489156d9582b19 |
| Source note | uspto-grants-1996_07 |