HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21471989, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 153025-28-6 | HCID 21471781 | — |
| Reactant | HCID 21472058 | HCID 21472058 | — |
| Product | HCID 21471989 | HCID 21471989 | 43.1% |
Reaction Steps
The reaction and procedure were conducted in a similar manner as in Example 24 using 0.9 g of 6-acetyl-2-(2-chloroethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine and 1.0 g of 4-(5-chloro-1,2-benzisoxazol-3-yl)piperidine hydrochloride to give 0.7 g of 6-acetyl-2-(2-(4-(5-chloro-1,2-benzisoxazol-3-yl)piperidin-1-yl)ethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine as an oil, m.p. 122°-124° C. (decomposition) as a hydrochloride thereof.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05532240 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-5be703cff7b84aa0a6d49bc965aeb572 |
| Source note | uspto-grants-1996_07 |