Chloroformamidinium chloride → HCID 19040784, compound

HRID 1734156Notes

Reaction equation

HRID 1734156 reaction equation
[NH2:1][C:2]1[C:7]([C:8]#[N:9])=[N:6][C:5]([C:10]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)=[O:11])=[C:4]([CH3:18])[N:3]=1.Cl.Cl[C:21]([NH2:23])=[NH:22]>COCCOCCOC>[NH2:23][C:21]1[N:22]=[C:8]([NH2:9])[C:7]2[C:2](=[N:3][C:4]([CH3:18])=[C:5]([C:10]([C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=3)=[O:11])[N:6]=2)[N:1]=1

Participants

4

Reactant 2

HCID 3084509Chloroformamidinium chlorideHCID 19040795HCID 19040795, compound

Product 1

HCID 19040784HCID 19040784, compound

Reagents, catalysts & solvents 1

HCID 8150DiglymeSolvent

Procedure

This compound is prepared in a manner analogous to that of Step C of Example 7, using 2.1 grams (0.009 mole) of 2-amino-3-cyano-6-methyl-5-phenylcarbonylpyrazine and 0.9 gram (0.009 mole) chloroformamidine hydrochloride in 20 mL of diglyme, yielding 2,4-diamino-7-methyl-6-phenylcarbonylpteridine.

Workup

  1. customThis compound is prepared in a manner analogous to that of Step C of Example 7

Sources & evidence

ORD record
ord-53c25ce7e3974d38bb5f33fceb57db95
Source dataset
uspto-grants-1996_07
Patent number
US05532367

Reaction notes

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