HRID1734254

反应详情

EQUATION

反应方程式

HRID 1734254 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

5-Benzyloxy-2-(N,N-dimethylamino) methyl-4-pyridone 1.0 g) in methanol (15 ml) was subjected to catalytic reduction with 10% palladium on activated carbon (200 mg) at atmospheric pressure. After removal of catalyst, the solution was concentrated under reduced pressure to give 2-(N,N-dimethylamino) methyl -5-hydroxy-4-pyridone (0.96 g).

WORKUP

后处理

  1. customAfter removal of catalyst
  2. concentrationthe solution was concentrated under reduced pressure