Hydrochloric Acid → HCID 22399715, compound

HRID 1734285Notes

Reaction equation

HRID 1734285 reaction equation
[ClH:1].C(O[NH:7][CH:8]([Si:18]([CH3:21])([CH3:20])[CH3:19])[C:9](=C=O)[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)(C)(C)C>C(OCC)C>[ClH:1].[CH3:20][Si:18]([CH3:19])([CH3:21])[CH:8]([NH2:7])[CH2:9][C:10]1[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 86749607HCID 86749607, compound

Product 1

HCID 22399715HCID 22399715, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent2×

Procedure

A 3N solution of HCl in diethyl ether (3 ml) was added at room temperature to a mixture of N-tertbutoxy-carbonyl-α-(trimethylsilyl)benzeneethanamine (0.150g, 0.51 mmol) in diethyl ether (3 ml). The mixture was stirred at room temperature for 48 hours. The resulting solid was filtered off and dried, invacuo, to yield 0.106 g of the expected α-(trimethylsilyl)-benzeneethanamine hydrochloride,

Workup

  1. filtrationThe resulting solid was filtered off
  2. customdried

Sources & evidence

ORD record
ord-37cba5cdcb854f4ea2ad899d02baef98
Source dataset
uspto-grants-1996_07
Patent number
US05532397

Reaction notes

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