HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Piperidinecarboxylic acid → HCID 67734335, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Piperidinecarboxylic acid | HCID 3773 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Product | HCID 67734335 | HCID 67734335 | — |
Reaction Steps
1-acetylpiperidine-4-carboxylic acid 1-Acetylpiperidine-4-carboxylic acid is prepared by bringing a solution of piperidine-4-carboxylic acid in acetic anhydride to reflux for 2 hours and then stirring for 16 hours at room temperature. The solution is then concentrated and the residue is triturated in ether. The solid compound is recovered by filtration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05534517 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-f616d1410c614487a26b58b9946a0739 |
| Source note | uspto-grants-1996_07 |