Dimethylformamide → HCID 19437776, compound

Participants

Reaction Steps

440 mg (1.0 mmol) of 7-benzyloxy-3-bromo-1-(4-methoxybenzyl)-2-methylpyrrolo[2,3-d]pyridazine, 735 μl (1.2 mmol) of a 15% strength solution of n-butyllithium in hexane and 160 μl (1.2 mmol) of dimethylformamide are reacted in 25 ml of tetrahydrofuran as described for Example 2a. Yield: 36%, m.p.: 139°-145° C.

Provenance & Evidence