Diethylamine → HCID 19438200, compound

HRID 1734713Notes

Reaction equation

HRID 1734713 reaction equation
[CH2:1]([NH:5][C:6]1[N:11]=[C:10]([P:12]([O:17][CH2:18][CH3:19])(=[O:16])[O:13][CH2:14][CH3:15])[N:9]=[C:8](P(OCC)(=O)OCC)[N:7]=1)[CH2:2][CH2:3][CH3:4].[CH2:28]([NH:30][CH2:31][CH3:32])[CH3:29]>>[CH2:1]([NH:5][C:6]1[N:7]=[C:8]([N:30]([CH2:31][CH3:32])[CH2:28][CH3:29])[N:9]=[C:10]([P:12]([O:13][CH2:14][CH3:15])(=[O:16])[O:17][CH2:18][CH3:19])[N:11]=1)[CH2:2][CH2:3][CH3:4]

Participants

3

Reactant 2

HCID 8021DiethylamineHCID 19438218HCID 19438218, compound

Product 1

HCID 19438200HCID 19438200, compound

Procedure

Tetraethyl 2-n-butylamino-1,3,5-triazine-4,6-diphosphonate prepared as described in Example 17 was dissolved in excess diethylamine and heated at reflux (59°-60° C.) for 6 hours to produce diethyl 2-n-butylamino-4-diethylamino-1,3,5-triazine-6-phosphonate.

Workup

  1. temperatureheated
  2. temperatureat reflux (59°-60° C.) for 6 hours

Sources & evidence

ORD record
ord-aba630ecb0f94c839bcd499c0102c6f3
Source dataset
uspto-grants-1996_07
Patent number
US05534573

Reaction notes

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