Methanol → HCID 19438424, compound

HRID 1734766Notes

Reaction equation

HRID 1734766 reaction equation
[CH2:1]([C:3]1([CH2:10][O:11][C:12](=[O:15])[CH:13]=[CH2:14])[CH2:8][O:7][C:6](=[O:9])[O:5][CH2:4]1)[CH3:2].C1(C)C=CC(S(O)(=O)=O)=CC=1.[CH3:27][OH:28]>>[CH2:1]([C:3]([CH2:10][O:11][C:12](=[O:15])[CH:13]=[CH2:14])([CH2:8][O:7][C:6]([O:5][CH3:4])=[O:9])[CH2:27][OH:28])[CH3:2]

Participants

4

Reactant 3

HCID 887MethanolHCID 6101p-Toluenesulfonic acidHCID 19438431HCID 19438431, compound

Product 1

HCID 19438424HCID 19438424, compound

Procedure

Analogous to Example 1, the title compound was synthesized using 21.4 g of 5-ethyl-5-acryloyloxymethyl-2-oxo-1,3-dioxane, 96 g of methanol and 0.1 g of p-toluenesulfonic acid.

Sources & evidence

ORD record
ord-fa73053a16324cae8354427431b9fc0d
Source dataset
uspto-grants-1996_07
Patent number
US05534647

Reaction notes

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