Methyl di-t-butyl hydroxyhydrocinnamate → HCID 19438411, compound

HRID 1734770Notes

Reaction equation

HRID 1734770 reaction equation
Cl[P:2]1[N:5]([C:6]2[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=2)[P:4](Cl)[N:3]1[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1.[C:19]([C:23]1[CH:24]=[C:25]([CH:32]=[C:33]([C:36]([CH3:39])([CH3:38])[CH3:37])[C:34]=1[OH:35])[CH2:26][CH2:27][C:28]([O:30][CH3:31])=[O:29])([CH3:22])([CH3:21])[CH3:20]>C(N(CC)CC)C>[C:19]([C:23]1[CH:24]=[C:25]([CH2:26][CH2:27][C:28]([O:30][CH3:31])=[O:29])[CH:32]=[C:33]([C:36]([CH3:39])([CH3:38])[CH3:37])[C:34]=1[O:35][P:2]1[N:5]([C:6]2[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=2)[P:4]([O:35][C:34]2[C:23]([C:19]([CH3:22])([CH3:21])[CH3:20])=[CH:24][C:25]([CH2:26][CH2:27][C:28]([O:30][CH3:31])=[O:29])=[CH:32][C:33]=2[C:36]([CH3:39])([CH3:38])[CH3:37])[N:3]1[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)([CH3:21])([CH3:22])[CH3:20]

Participants

4

Reactant 2

HCID 62603Methyl di-t-butyl hydroxyhydrocinnamateHCID 15389826HCID 15389826, compound

Product 1

HCID 19438411HCID 19438411, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

The procedure of Example 1 is repeated using 2,4-dichloro-1,3-diphenyl-1,3,2,4-diazadiphosphetidine, methyl 3,5-di-tert-butyl-4-hydroxyhydrocinnamate and triethylamine to give the title compound.

Sources & evidence

ORD record
ord-6e00ae742178433996b8f2b8a21ab20e
Source dataset
uspto-grants-1996_07
Patent number
US05534646

Reaction notes

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