Octadecyl DI-tert-butyl-4-hydroxyhydrocinnamate → HCID 19438410, compound

HRID 1734771Notes

Reaction equation

HRID 1734771 reaction equation
Cl[P:2]1[N:5]([C:6]2[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=2)[P:4](Cl)[N:3]1[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1.[C:19]([C:23]1[CH:24]=[C:25]([CH:49]=[C:50]([C:53]([CH3:56])([CH3:55])[CH3:54])[C:51]=1[OH:52])[CH2:26][CH2:27][C:28]([O:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH2:47][CH3:48])=[O:29])([CH3:22])([CH3:21])[CH3:20]>C(N(CC)CC)C>[C:19]([C:23]1[CH:24]=[C:25]([CH2:26][CH2:27][C:28]([O:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH2:47][CH3:48])=[O:29])[CH:49]=[C:50]([C:53]([CH3:55])([CH3:54])[CH3:56])[C:51]=1[O:52][P:2]1[N:5]([C:6]2[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=2)[P:4]([O:52][C:51]2[C:23]([C:19]([CH3:22])([CH3:21])[CH3:20])=[CH:24][C:25]([CH2:26][CH2:27][C:28]([O:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH2:47][CH3:48])=[O:29])=[CH:49][C:50]=2[C:53]([CH3:54])([CH3:56])[CH3:55])[N:3]1[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)([CH3:20])([CH3:21])[CH3:22]

Participants

4

Reactant 2

HCID 16386Octadecyl DI-tert-butyl-4-hydroxyhydrocinnamateHCID 15389826HCID 15389826, compound

Product 1

HCID 19438410HCID 19438410, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

The procedure of Example 1 is repeated using 2,4-dichloro-1,3-diphenyl-1,3,2,4-diazadiphosphetidine, n-octadecyl 3,5-di-tert-butyl-4-hydroxyhydrocinnamate and triethylamine to give the title compound.

Sources & evidence

ORD record
ord-dab53666a09744cc9d64673d167a69b4
Source dataset
uspto-grants-1996_07
Patent number
US05534646

Reaction notes

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