2,4,6-Tri-tert-butylphenol → HCID 19438413, compound

HRID 1734772Notes

Reaction equation

HRID 1734772 reaction equation
Cl[P:2]1[N:5]([C:6]([CH3:9])([CH3:8])[CH3:7])[P:4](Cl)[N:3]1[C:11]([CH3:14])([CH3:13])[CH3:12].[C:15]([C:19]1[CH:24]=[C:23]([C:25]([CH3:28])([CH3:27])[CH3:26])[CH:22]=[C:21]([C:29]([CH3:32])([CH3:31])[CH3:30])[C:20]=1[OH:33])([CH3:18])([CH3:17])[CH3:16]>C(N(CC)CC)C>[C:15]([C:19]1[CH:24]=[C:23]([C:25]([CH3:28])([CH3:27])[CH3:26])[CH:22]=[C:21]([C:29]([CH3:32])([CH3:31])[CH3:30])[C:20]=1[O:33][P:2]1[N:5]([C:6]([CH3:9])([CH3:8])[CH3:7])[P:4]([O:33][C:20]2[C:21]([C:29]([CH3:30])([CH3:31])[CH3:32])=[CH:22][C:23]([C:25]([CH3:28])([CH3:27])[CH3:26])=[CH:24][C:19]=2[C:15]([CH3:18])([CH3:17])[CH3:16])[N:3]1[C:11]([CH3:14])([CH3:13])[CH3:12])([CH3:18])([CH3:17])[CH3:16]

Participants

4

Reactant 2

HCID 129022,4,6-Tri-tert-butylphenolHCID 125327951,3-Di-tert-butyl-2,4-dichloro-1,3,2,4-diazadiphosphetidine

Product 1

HCID 19438413HCID 19438413, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

The procedure of Example 1 is repeated using 2,4-dichloro-1,3-di-tert-butyl-1,3,2,4-diazadiphosphetidine, 2,4,6-tri-tert-butylphenol and triethylamine to give the title compound.

Sources & evidence

ORD record
ord-55dc06b118ee4b3291821c3c9277e819
Source dataset
uspto-grants-1996_07
Patent number
US05534646

Reaction notes

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