2,6-Di-tert-butyl-4-methylphenol → HCID 19438422, compound
Reaction equation
Cl[P:2]1[N:5]([C:6]2[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=2)[P:4](Cl)[N:3]1[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1.[C:19]([C:23]1[CH:28]=[C:27]([CH3:29])[CH:26]=[C:25]([C:30]([CH3:33])([CH3:32])[CH3:31])[C:24]=1[OH:34])([CH3:22])([CH3:21])[CH3:20]>C(N(CC)CC)C>[C:30]([C:25]1[CH:26]=[C:27]([CH3:29])[CH:28]=[C:23]([C:19]([CH3:22])([CH3:21])[CH3:20])[C:24]=1[O:34][P:2]1[N:5]([C:6]2[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=2)[P:4]([O:34][C:24]2[C:25]([C:30]([CH3:31])([CH3:32])[CH3:33])=[CH:26][C:27]([CH3:29])=[CH:28][C:23]=2[C:19]([CH3:22])([CH3:21])[CH3:20])[N:3]1[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)([CH3:33])([CH3:32])[CH3:31]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
The procedure of Example 1 is repeated using 2,4-dichloro-1,3-diphenyl-1,3,2,4-diazadiphosphetidine, 2,6-di-tert-butyl-4-methylphenol and triethylamine to give the title compound.
Sources & evidence
- ORD record
- ord-c9eb5712ee6a4a7bbb45008346a9639b
- Source dataset
- uspto-grants-1996_07
- Patent number
- US05534646
Reaction notes
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