HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 19068938, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Methyl Thioglycolate | HCID 16907 | — |
| Reactant | HCID 19068948 | HCID 19068948 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19068938 | HCID 19068938 | — |
Reaction Steps
400 μl of methyl 2-mercaptoacetate was added to a slurry of 1050 mg of (80) and 1.1 g of K2CO3 in 10 ml of MeOH, and left with stirring for 48 hours. 20 ml of water was added, and the precipitate filtered off and dried. This material was thoroughly washed with pentane, filtered, dried, and recrystallized from EtOH giving 230 mg of (81) as a white powder. M.p. 85.4°-86° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05536721 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-f056c2fb395e4b6283d4abbfb15f5e5c |
| Source note | uspto-grants-1996_07 |