Pyridine → HCID 15838313, compound

Participants

Reaction Steps

To 17β-(4-aminophenoxy)-4-methyl-5α-4-azaandrostan-3-one hydrochloride (7mg) in CH2Cl2 (100 μl) was added acetic anhydride (30 μl) followed by adding pyridine (50 μl). The mixture was stirred at room temperature for 2 hr and then concentrated to dryness. The residue was purified via a silica gel plate developed with 5% MeOH--EtOAc (Rf =0.3) to give the title product, mp. 340° C.

Provenance & Evidence