HCID 15838328, compound → HCID 86749639, compound

Participants

Reaction Steps

The product of Step D, above, and platinum oxide (35 mg) in glacial acetic acid (2 ml) was hydrogenated at 40 psi for 22.5 hours. The mixture was filtered through a pad,of celite. The filtrate was concentrated and the residue purified via preparative TLC using one silica gel plate (1000μ) developed with EtOAc to give the title product (Rf =0.22; mp 170°-172° C.).

Provenance & Evidence