HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 19437009, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | HCID 12446018 | HCID 12446018 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 19437009 | HCID 19437009 | 92.6% |
Reaction Steps
Following the same procedure as in Example 44 Step A, 5 g (19 mmol) of dimethyl-(4-chlorobutyl)-phenylsilane in 150 ml of acetone are refluxed for 60 hours with 17 g (114 mmol) of sodium iodide to afford 5.6 g (83%) of expected dimethyl-(4-iodobutyl)-phenylsilane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05536732 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-6be57eb2b47e48ff905fce5897f84285 |
| Source note | uspto-grants-1996_07 |