HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10532610, compound → HCID 10626499, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10532610 | HCID 10532610 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 10626499 | HCID 10626499 | 72% |
Reaction Steps
To a solution of 8.10 g of the intermediate obtained from Step A in 80 mL of ethanol was added 1 g of 20% palladium hydroxide/C and hydrogenated with hydrogen balloon for 1 h. The catalyst was filtered off through a pad of celite and washed with ethyl acetate. The filtrate was concentrated to give 4.69 g of the product as a colorless foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05536716 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-b5e3fe2d7f5244be8b59d192edc39cc4 |
| Source note | uspto-grants-1996_07 |