Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
p-Methoxybenzophenonoxime → 1-(4-Methoxyphenyl)-1-phenylmethanamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | p-Methoxybenzophenonoxime | HCID 185567 | — |
| 반응물 | Ammonium Acetate | HCID 517165 | — |
| 반응물 | Sodium cyanoborohydride | HCID 5003444 | — |
| 촉매 | titanium(III) trichloride | HCID 10313229 | — |
| 생성물 | 1-(4-Methoxyphenyl)-1-phenylmethanamine | HCID 350041 | 76.9% |
반응 단계
Following a procedure similar to that described in Preparation 12, but using 9.4 g of 4-methoxybenzophenone oxime, 33.9 g of ammonium acetate, 7.46 g of sodium cyanoborohydride, and 79 ml of a 17-19% by volume aqueous solution of titanium trichloride, 6.78 g of the title compound were obtained as an oily substance.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05536714 |
| 출처 데이터셋 | uspto-grants-1996_07 |
| ORD ID | ord-8590e83fe4994ba288f6cd8734966070 |
| 출처 메모 | uspto-grants-1996_07 |