Lithium Hydroxide → Lithium p-trifluoromethylsulfonyl phenolate

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Reaction Steps

Compound (2) from Example 2, in anhydrous methanol, was neutralized with equivalent amount of lithium hydroxide: The solvent was then removed, and the residue dissolved in a small amount of anhydrous THF. Ether was subsequently added and the solution stored in a refrigerator. The precipitated crystals were filtered and washed with ether.

Provenance & Evidence