HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperazine, 1-(3-chloropropyl)-4-phenyl- → HCID 13536258, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperazine, 1-(3-chloropropyl)-4-phenyl- | HCID 139197 | — |
| Reactant | HCID 13536191 | HCID 13536191 | — |
| Product | HCID 13536258 | HCID 13536258 | — |
Reaction Steps
In the same manner as in Reference Example 1, methyl 7-chloro-3-oxo-3,4-dihydro-2H-1,5-benzoxathiepine-4-carboxylate was reacted with 3-(4-phenylpiperazin-1-yl)propyl chloride to give methyl 7-chloro-3-oxo-4-[3-(4-phenylpiperazin-1-yl)propyl]3,4-dihydro-2H-1,5-benzoxathiepine-4-carboxylate. When converted to hydrochloride, white crystals were obtained, melting point 197°-199° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05538974 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-357c34ae590d472687827abc5b08aecc |
| Source note | uspto-grants-1996_07 |