1-Heptanamine → HCID 22862769, compound

HRID 1735926Notes

Reaction equation

HRID 1735926 reaction equation
[CH2:1]([NH2:8])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH3:7].[O:9]=[CH:10][C@@H:11]([C@H:13]([C@@H:15]([C@@H:17]([CH2:19][OH:20])[OH:18])[OH:16])[OH:14])O>O>[CH2:1]([NH:8][CH:19]1[O:20][C@H:11]([CH2:10][OH:9])[C@@H:13]([OH:14])[C@H:15]([OH:16])[C@H:17]1[OH:18])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH3:7]

Participants

4

Reactant 2

HCID 81271-HeptanamineHCID 107526(2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal

Product 1

HCID 22862769HCID 22862769, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A solution of heptylamine (11.5 g in 50 ml of ethanol) was added to a solution containing 9 g of glucose and 35 ml of water. The reaction mixture was stirred for about 24 hours at ambient temperature. The precipitate formed was filtered and recrystallized from ethanol, then lyophilized.

Workup

  1. customThe precipitate formed
  2. filtrationwas filtered
  3. customrecrystallized from ethanol

Sources & evidence

ORD record
ord-cc516f589de14ac8bf843b50c3645a28
Source dataset
uspto-grants-1996_07
Patent number
US05539091

Reaction notes

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