HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Benzyl 3-aminopropanoate hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Benzyl 3-(Boc-amino)propanoate | HCID 10468829 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | Benzyl 3-aminopropanoate hydrochloride | HCID 19434764 | — |
Reaction Steps
Compound (25) (517 mg, 1.85 mmol) was treated with 4N HCl in dioxane at room temperature for 2 h. The reaction mixture was evaporated at reduced pressure, evaporated from toluene and then dried under vacuum to give crude benzyl β-alaninate hydrochloride which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05539104 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-5ad46b5c7d7f4e1fabd57046cb35abc6 |
| Source note | uspto-grants-1996_07 |