HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19434127, compound → HCID 54017237, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19434127 | HCID 19434127 | — |
| Reactant | Trimethylorthoacetate | HCID 21927715 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 54017237 | HCID 54017237 | 167.8% |
Reaction Steps
The product from Step D (1.6 g, 4.32 mmol) was dissolved in dry acetonitrile (20 mL) and trimethylorthoacetate (11 mL) was added. The mixture was heated at reflux temperature for 18 hr and then evaporated to provide an oil (1.88 g, 100%) which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05538966 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-fb6c10520bc24f9bae103a4c7e4e5a10 |
| Source note | uspto-grants-1996_07 |