HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 9817398, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 10503983 | HCID 10503983 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 9817398 | HCID 9817398 | 64.6% |
Reaction Steps
1.42 g of Compound 11 was dissolved in 84 ml of dioxane, 36 ml of concentrated hydrochloric acid was added and the mixture was heated at reflux for 3 hours. The reaction solution was cooled on ice and the precipitated crystals were collected by filtration to give 579 mg (57%) of Compound 12.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05539112 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-8919be3ab7384c93a122fe73dca0aae4 |
| Source note | uspto-grants-1996_07 |