Sodium Tetraphenylborate → HCID 86749660, compound

HRID 1736257Notes

Reaction equation

HRID 1736257 reaction equation
[Br-].[CH3:2][C:3]1[CH:17]=[CH:16][C:6]([C:7](=[O:15])[CH2:8][N+:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)=[CH:5][CH:4]=1.[C:18]1([B-:24]([C:37]2[CH:42]=[CH:41][CH:40]=[CH:39][CH:38]=2)([C:31]2[CH:36]=[CH:35][CH:34]=[CH:33][CH:32]=2)[C:25]2[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=2)[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1.[Na+]>>[C:37]1([B-:24]([C:18]2[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=2)([C:25]2[CH:26]=[CH:27][CH:28]=[CH:29][CH:30]=2)[C:31]2[CH:36]=[CH:35][CH:34]=[CH:33][CH:32]=2)[CH:38]=[CH:39][CH:40]=[CH:41][CH:42]=1.[CH3:2][C:3]1[CH:4]=[CH:5][C:6]([C:7](=[O:15])[CH2:8][N+:9]2[CH:10]=[CH:11][CH:12]=[CH:13][CH:14]=2)=[CH:16][CH:17]=1

Participants

3

Reactant 2

HCID 2723787Sodium TetraphenylborateHCID 12266212HCID 12266212, compound

Product 1

HCID 86749660HCID 86749660, compoundYield 100%

Procedure

The title compound was prepared similarly to Example 2 from 4-methylphenacylpyridinium bromide and sodium tetraphenylborate in a yield of 100%.

Sources & evidence

ORD record
ord-4bf0ae433dfa4084ad66248986730e9e
Source dataset
uspto-grants-1996_07
Patent number
US05541032

Reaction notes

Loading…