Sodium Tetraphenylborate → HCID 86749661, compound

HRID 1736260Notes

Reaction equation

HRID 1736260 reaction equation
[Br-].[CH3:2][O:3][C:4]1[CH:18]=[CH:17][C:7]([C:8](=[O:16])[CH2:9][N+:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)=[CH:6][CH:5]=1.[C:19]1([B-:25]([C:38]2[CH:43]=[CH:42][CH:41]=[CH:40][CH:39]=2)([C:32]2[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=2)[C:26]2[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=2)[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1.[Na+]>>[C:38]1([B-:25]([C:19]2[CH:20]=[CH:21][CH:22]=[CH:23][CH:24]=2)([C:26]2[CH:27]=[CH:28][CH:29]=[CH:30][CH:31]=2)[C:32]2[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=2)[CH:39]=[CH:40][CH:41]=[CH:42][CH:43]=1.[CH3:2][O:3][C:4]1[CH:5]=[CH:6][C:7]([C:8](=[O:16])[CH2:9][N+:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)=[CH:17][CH:18]=1

Participants

3

Reactant 2

HCID 2723787Sodium TetraphenylborateHCID 117093181-[2-(4-Methoxyphenyl)-2-oxoethyl]pyridin-1-ium bromide

Product 1

HCID 86749661HCID 86749661, compoundYield 100%

Procedure

The title compound was prepared similarly to Example 2 from 4-methoxyphenacylpyridinium bromide and sodium tetraphenylborate in a yield of 100%.

Sources & evidence

ORD record
ord-e1eab50e6e744047b451cd439a62f24b
Source dataset
uspto-grants-1996_07
Patent number
US05541032

Reaction notes

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