HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Phenyl-1H-imidazol-5-yl)methanol → HCID 19973549, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Phenyl-1H-imidazol-5-yl)methanol | HCID 20253759 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 19973549 | HCID 19973549 | 70.8% |
Reaction Steps
1,4-Dioxane (10 ml) was mixed with 1 g of (4-phenyl-1H-imidazol-5-yl)methyl alcohol and 3 g of activated manganese dioxide. The obtained mixture was treated at 80° C. for 30 minutes to conduct a reaction. The reaction mixture was passed through a hot filter and the filter cake was washed with acetone. The washings and the filtrate were combined and concentrated to give 0.7 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05541213 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-1d0ccdf2d34941c5830bb3da0c7a2c75 |
| Source note | uspto-grants-1996_07 |