Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Valeryl chloride | HCID 61186 | — |
| Reactant | 4-Methoxy-2-nitroaniline | HCID 66793 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 4184921 | HCID 4184921 | — |
Reaction Steps
4.2 g (0.025 mol) of 2-nitro-4-methoxy-aniline are dissolved in 30 ml of pyridine, cooled to 0° C. and treated with 3.3 g (0.0275 mol) of valeryl chloride with stirring. After stirring for 1 hour at ambient temperature, the mixture is poured into iced water, the crystals are filtered off under suction and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05541229 |
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| Source dataset | uspto-grants-1996_07 |
|---|
| ORD ID | ord-1c890ec182e64bada1bcec7e25b7e916 |
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| Source note | uspto-grants-1996_07 |
|---|
